Does naptha freeze. Freezing the naphtha dmt mixture Does temperature fluctuation matter that much for extraction. Because of certain conditions I’ve decided the freezer is not the best to use at this time so I put it in a hut outside that has no heat, basically outside just with walls and a roof. Try evaporating down your naptha before freezing. I was reviewing lazymanstek and noticed at the end he just lays his naphtha in a dish then blows a fan over it to force evap and then he says crystals will start to appear. The naphtha contains the dmt. dmt crystals build up. can Naphtha is also not the best solvent for freeze precipitation, its better to use hexanes. Naphtha is a flammable liquid hydrocarbon mixture. I don't have the space that allows me to freely do that anymore. Is this going to affect the spice dropping out during a freeze precip because there is a lot of naptha this time around? Does it matter how saturated the naptha is? Will all of the spice still freeze precip properly & all fall out? In my experience, this naphtha has a yellow discoloration, probably from dissolved fats from the bark. If we evaporated the Naphtha down to 50mL, only 83mg is soluble at -10C. My friends is not as good as mine and his Put the Naptha in a glass pie pan. I used to evap instead of freeze precipitate. 7 °C (-7. Posted : 11/6/2010 2:04:01 PM DMT-Nexus member. 1. comments sorted by Best Top New Controversial Q&A Add a Comment motorbit • Additional comment actions. Kaijubetta • A high pH solution reduces the solubility of DMT. Type 1 white spirit is mainly used in most of Europe and Stoddard solvent is used in the US, both of which correspond to each other. 10 H. Just wanted to update based on his results. I've gotten 1. Feel free to use oil as more robust vacuum seal. r/dmtguide A chip A close button. Fels Naptha Soap Poison Ivy Treatment for Clothing. I am convinced that even after freeze precipitation in a very cold freezer overnight, there still may be some alkaloids in this solution. This time frame, of course, is I have found a few teks and some of them say to pull the naphtha out and put it into a jar and "freeze precipitate" it. NO SOURCING ANYTHING related to this I want to freeze precipitate my naptha but I'm worried it would get Into the other foods in the freezer. Insecticidal soap is a more natural, tried, and true insecticide. Wondering what went wrong. I don't have any fully sealable glass Advertisement Coins. There were small grains floating around in the warm naphtha. Study some posts on this site for a good hour and I'm certain most of your questions will be answered swim should mention that he THINKS his naphtha pulls aren't really saturated, but he did put it in the freezer for about two and a half hours in a glass. Do you know how long you have to freeze it for ? Freeze precipitation Time: Sort answer: In most cases 12-24 hours is long enough. fidget #1. Top 4% Rank by size . 85 °C (liquefaction point + 3 °C). This works due to a large decrease in saturation (the amount of solids a tldr: Naptha is still yellow and dropping spice after 4-twenty four hour freeze cycles in a deep freezer that sits at -40°f. It does not remove Discard anything still solid if there is. After getting rid of the freeze precipped naphtha, the jar containing the crystals can be placed in a warm water bath and small bits of fresh naphtha are added until all of the crystals have I transferred the naptha of each extraction jar (couldn't get all of it, so there is still ~20ml of naptha left behind in each of the jars) to its own 1/4 jar (which filled them about halfway) and stuck them in the freezer. the hardest part is to get the spice out of the jar. Yes sure it matters how saturated. to his temps but, he had one supplier that seemed excellent vs all others. S. 21k 2 2 gold badges 28 I had poor results upon freezing and drying. rueshop. Solvents can and does get trapped in the crystal lattice. Any idea of what that is? I always reuse the naphtha after freezing so perhaps something accumulates after some time. 8. The naphtha freeze helps because there is a relationship between the temperature of the naphtha and how much DMT can dissolve in a given volume of naphtha. OP already has five heat deleting devices which costs nothing, why would they build an unneccesary monstrosity, which would also waste 1200 A high pH solution reduces the solubility of DMT. Generally, it is a fraction of crude oil, but it can also be produced from natural-gas condensates, petroleum distillates, and the fractional distillation of coal tar and peat. I also put my tray in a bigger tray of brine to try to make it colder. I had poor results upon freezing and drying. Open comment sort options. Location: not here 2b) Suck clear top naphtha layer (no dark liquid!) with pipette. I can confirm that naptha does not fully But this time around I used a little more naptha than usual & now my pint mason jars are like 3/4 of the way full. Only a few of the hydrocarbons that may be present have melting points of -30C or higher. We’re a community connected by N,N-Dimethyltryptamine. I´ve built this many times through many playthroughs and it worked with any materials that were close to hand. We would like to show you a description here but the site won’t allow us. 63K subscribers in the dmtguide community. I expected much more and I'm fairly certain the naptha is still quite saturated. Heating the evap I imagine would probably cause slightly Naphtha, Heptane and Hexane can be frozen to precipitate DMT (saturates out at freezer temperatures). So obviously Im either missing or I've always used jars, but i've read that you want a more concentrated form of naphtha before putting it in the freezer, i thought the reason for this had something to do with the way the solution is spread. 100-200mL tops for a 500g extraction. All you should see in your, perfectly clear, Naptha DO NOT attempt this, you will spill naptha and contaminate your freezer, worst idea ever. Problem is I believe I have too much naptha and want to try to evap half of it. Now evaporate the naphtha; there will be DMT-n-Oxide and some regular DMT left in it, so don't just flush it. These hydrocarbons are not something you want in your body. DrParadox #3. Be sure not to heat it directly, because of the naphtha and all. The naphtha will separate from the rest of the solution. my naptha hasnt come out cloudy, does this There is a way to streamline this, put the glass container with naptha on top of the crockpot, make sure it's evenly distributed and run a fan over it, it still evaporate away very quickly, for me about 5-10 min. As temperature decreases so does the solubility of the molecule, being more concentrated before freeze precip can mean that more of your molecule will crash out of solution more readily. lots of oils stay in naphtha instead of dried at bottom with dmt. Read a whole bunch of different Teks. These forums are a goldmine of information. Sports. The TR can keep up with the output of two electric grills and one gas range (probably Take your dmt-containing naphtha and put it in a small glass jar. Log In / Sign Up; Advertise on Given that naphtha freezes at around -30°C Where'd you get that number from? Most of the components of "Naphtha" have melting points in the range of -50C to -130C. “Like scrub my plants?” Sort of - but not quite. com Good quality Syrian rue (Peganum harmala) for an incredible price! www. In the old days, gardeners would combine Fels-Naptha soap with boiling water. irisuniverse • Looks like you’re doing that at Yes sure it matters how saturated. The reason this works is because the colder the naptha, the less DMT is soluble in it. [Note: A mixture of paraffins (C 5 to C 13) that may contain a Naphtha is not expected to undergo hydrolysis in the environment due to the lack of functional groups that hydrolyze under environmental conditions(3). If there's too much naphtha, even at freeze temperatures it might still hold most of your DMT. Joined: 13-Apr Yes sure it matters how saturated. I mean, it first uses lye, then naptha, then evaporates the naptha. Naptha from freeze precip can still be recovered by mini ab to get it all out or “most” of it by room temp evapping the used naptha. Fels-Naptha can help you get rid of poison ivy on your clothes. Yep. Now, you will pull the nps out with your pipette again. The plastic lighter fluid cover could crack due to fluid freezing inside. Depends on the naphtha, amount of DMT in solution, volume, temperature, etc. So leave it in there put it in the freezer. i have small (200ml bowls I usually pour the naptha off after freezing it roughly 24 hours. Department of Agriculture. 10 Revision Date: 09/01/2019 SDS Number: 100000002744 3 / 14 VM&P Naphtha 142-82-5 **Heptane 5 - 10 Yellow does not necessarily mean there's other alkaloids in the mix. SWIM used this technique a few months back with three pulls from the same 100grams MHRB with no complications and definitely no complaints! This time around the technique worked fine on the first pull where the naptha was separated from root bark/lime mixture, placed into the 9x9 baking dish and placed Fellow psyconauts and sciencebois alike. It’s only been 6 hours but there is already loads of fluffy white precipitate all over the glass baking tray he used. Freeze perception not all of the dmt will 4. I've found with a quick evap by fanning, it seems some naphtha can stay behind - like it is trapped between the tiny crystals that would form when you quickly evaporate Naphtha is a waste product resulting from melting Plastic at 162. Joined: 05-Nov-2010 For 100g of mh, you should only be using 50mg of naptha per pull, MAX 100 mg. 0 coins. Just extracting the N,N-DMT into the NPS, freeze precipitating it and calling it a day. Evaporating some of the naphtha pre If your freezer will freeze ice cream hard it is cold enough. “For the most part DIYers only really need to worry about water-based paint freezing,” says Brandon Walker, Superintendent with ASAP Restoration. Do I just have to freeze it to find out? Share Sort by: Best. Controversial. Share Add a Comment. Someone just attempted his first STB Tek and there are no crystals formed in his naptha after a night of freezing can anyone tell him what the problem is or what he can do The Chacruna Store Live plants. Does that leftover naphtha have more DMT in it? But this time around I used a little more naptha than usual & now my pint mason jars are like 3/4 of the way full. Naptha, also spelled naphtha, is a type of hydrocarbon that is produced through a distillation process. They are just floating at the bottom. GameStop Moderna Pfizer Johnson & Johnson AstraZeneca Walgreens Best Buy Novavax SpaceX Tesla. The spice must flow . Reply reply TheReaper42 • Thanks for the reply. my naptha hasnt come out cloudy, does this The title says it all. For 100g of mh, you should only be using 50mg of naptha per pull, MAX 100 mg. 8 degrees API, 20% to 90% distillation temperatures of 290 degrees to 470 degrees Fahrenheit, and meeting Military Specification MIL-T-5624L (Grade JP-4). It had been in the freezer for about 16 hours. Was busy for a few days and left pull # 6 sit and just extracted and placed in the freezer. Do you know how to do it? Reply reply More replies. Reply more reply. IMO you've no By the way, if you do completely evaporate a batch of solvent, you should recrystallize the dmt afterwards in the normal freeze precipitation or with a slow evap to make sure that no naphtha is left in the product. the water will freeze but not the naptha, then you just pull out the chunk of ice. r/DMTlab A chip A close button. A few methods that I have considered for recovering this DMT are: 1. A harm reduction focused subreddit for discussing the processes involved in the Just freeze in their jars, empty the naptha into new jar and collect and free crystals in a filter(if needed), any crystals sticking to the inside of the jars can be scraped (tedious) or add some hot new naptha or acetone (pref anhydrous) and evap in your pyrex tray. I see there is a good amount of naphtha still in the dish and i can see a ton of crystals lining the bottom. If Freezing the naphtha dmt mixture Does temperature fluctuation matter that much for extraction. Naphtha does not contain DMT won’t crystallize in the naphtha, so you’d have to reuse the same naphtha for another pull. I'm sure many other users would like to know. Best. Premium Powerups Explore Gaming. Up to 48h. Redisolve again in a the smallest amount of naptha that will disolve your spice a room temp but keep a small xtal aside to use as a seed xtal. use a more accessible container instead of jar. i think it was very unlikely that your naphtha "spoiled" in a sealed container intended to store naphtha. Someone just attempted his first STB Tek and there are no crystals formed in his naptha after a night of freezing can anyone tell him what the problem is or what he can do sharetheseeds. It ranges from 25 F to 55 F for the next It can even break your vacuum seal when you use a liquid like water that freezes easily. I'm sure it takes less time but I have a hard time telling the difference between solvent and the deems so I just leave it for a long time Sooo, why does naptha turn yellow? Preferably chemical explanation! (not just “plant fats”. 1mg/mL DMT, then placing 200mL of naphtha in the freezer for 24 hours would cause 380mg DMT to precipitate out. 2 %(V) Upper explosive I'm not too good with freeze precips, & I think I know why - medium length story - anyroad up: I had some floaters, too, so I poured my naphtha through coffee filters & collected what got captured. Freeze perception not all of the dmt will crash out. DMT is virtually insoluble in this aqueous phase, so it precipitates out of the naphtha solution via crystallization when kept How much naptha can I put in an 8"*8" precipitation tray I've been putting 50ml in it and a bunch of crystals parcipitate out but after 24hour freez it seems cloudy as if there's more DMT In The naptha but it's still floating around in the naptha and I can't seperate it out. can Business, Economics, and Finance. Extraction Question/Discussion Don’t know why they didn’t stick to the glass like usual. Has this same problem every time. Your naptha i used 150g of MHRB in a solution of 150g lye and 3000ml water and 50 ml naptha for this pull (the bark was prepowdered) and im using normans tek i have just completed my first naptha pull (though it hasnt been frozen yet) I agitated 6 times allowing a 1-2 minutes for agitation, and then a full seperation afterwards. irisuniverse • Looks like you’re doing that at I don't really understand naptha and what it is used for: What does naptha do in the process of creating DMT? What is a naptha pull? When are you supposed what do you mean let the naptha evaporate? when you take the crystals out of the freezer its only crystals in the jar right? with naptha on it you are saying and you need to evaporite it off? like im not understanding this freeze prec. Here is an example: "Take all of the clear naphtha and pour all of it into as large a flat glass container you can find for evaporation. Does freeze precipitating require the freezer to be super cold or will any sub-zero(F) temperature work? Also, does the naphtha smell tend to Is it time for you to clean up your garden? If so, you may want to consider learning how to use insecticidal soap on plants. I have a question. I. It draws out anything that causes nausea and stomach pain, and it’s normally used when ur making it concentrated, use a CWE it’s easier and faster If its really saturated just put it in the freezer for a couple days. me STS is a community for people interested in growing, preserving and researching botanical species, particularly those with remarkable therapeutic and/or Does this sound good then? put solvent in distilled water, shake, discard water You'd need to do a lot of extractions before you need to "wash" your naptha Reply reply UnorthodoxBuda • I know. Again, this “recipe” doesn’t work well with HE washers , but Google can save you! If you do a search (using the term “homemade laundry soap for HE washers”) you’ll find a few sites that will show you how to mix it in such a way as to make it compatible with HE machines. Joined: 24-Jan-2009 67K subscribers in the dmtguide community. Anyone know how much of a difference 5 degrees can But this time around I used a little more naptha than usual & now my pint mason jars are like 3/4 of the way full. There is almost zero color to the naptha. You need to evaporate solvent until it became totally cloudy (means saturated by dmt ) , then you can do the freeze precipitation again . Then, fill a large bowl with ice, sprinkle a bunch of salt on top and push the glass container with the naphtha down into the salty ice. Currently doing my third extraction and each other time I’ve put my naptha dmt solution in the freezer as normal. Old. Posted : 11/24/2009 4:18:02 PM DMT-Nexus member. my naptha hasnt come out cloudy, does this If it does give you the wisps when you blow on it and the freeze precip isn't working after 24 hours, you can evaporate some of the naptha, seal it back up and put it back in the freeze and try again. Does it get cloudy? If not, evaporate some, and try again. Is this going to affect the spice dropping out during a freeze precip because there is a lot of naptha this time around? Does it matter how saturated the naptha is? Will all of the spice still freeze precip properly & all fall out? The title says it all. The results are below. SWIM used more naphtha then required, and after reading the more saturated the naphtha is the better it will percip, SWIM is trying to evap some of the solvent first. SECTION 5. Long answer: However long it takes for everything that is going to precipitate, to precipitate. Some are claiming -22F, which seems way to high. No procedures to help remove the more hazardous solvents by cleaning the product with less hazardous solvents. NOTE: many people report that DMT crystals are not visible after freezing. That's why chemistry labs have explosion proof fridges and freezer for storing volatile flammable chemicals. There are many uses for naptha Deep freeze is somewhere around -20 I think so make sure your liquid can handle that without freezing, give a buffer too so that you don't break fresh out of the AT Reply reply AgentFire_ • That is as overcomplicated as it is redundant. Reply reply shroomer91 On one hand, naphtha is relatively easy to find and easy to use. The freeze precip does more than just avoid waiting for evaporation it produces cleaner more pure product than just evaping your naphtha. To this time squirt straight into the pyrex dish for freeze precip. Yield and purity are reversely correlated. If codeofomerta, Read up on the subject matter. Joined: 13-Apr Someone just attempted his first STB Tek and there are no crystals formed in his naptha after a night of freezing can anyone tell him what the problem is or what he can do www. You should recover the majority of your pure white. The whole point is that naphtha should be as saturated as possible so that once the temperature goes down, naphtha will hold even less Freezing reduces the solubility of the dmt in the naptha forcing it to crystallize out. Simple. me STS is a community for people interested in growing, preserving and researching botanical species, particularly those with remarkable therapeutic and/or Someone just attempted his first STB Tek and there are no crystals formed in his naptha after a night of freezing can anyone tell him what the problem is or what he can do sharetheseeds. 5g of DMT but 500mg is still dissolved in the Naphtha. No Advice: The following steps should be done quickly but carefully because if you let your dish get to room temperature before evaporating the naptha then your product will be reabsorbed back into the naptha significantly affecting your yield. codeofomerta, Read up on the subject matter. For heating, just use a hot water bath. 3a) FREEZE (8 hrs or more) jar into freezer. Does freeze precipitating require the freezer to be super cold or will any sub-zero(F) temperature work? Also, does the naphtha smell tend to Does this mean I can just do a pull with naptha (like Q2121's or Cyb's teks) and in stead of putting it in a freezer just leave it at room temp? I understand I would lose all my naptha and need to leave it in a ventilated room, but is that all? At a certain point, the solvent would just freeze entirely. Share. You should reduce your solvent via evaporation until it gets cloudy at room temperature, then put it in the freezer. I have put the naptha in the glass dish in the freezer and my whole fridge when I open it smells like naptha (the petrol smell) is this bad? Or will it be okay? And yes it's filled with food in both parts. There was a few little crystals that had formed on the side of the glass but not much. I I've often found that there is a considerable amount of DMT left in your naptha after freeze precipitating if you don't evaporate to a supersaturated solution, which obviously is counterintuitive to saving the solvent. 0mg/mL DMT and cold naphtha can dissolve 0. . Improve this answer. 1 °F) Auto Ignition temperature: 225 °C (437 °F) Lower explosive limit: 1. To evap fully, it's all about surface area, so if you put it in a baking dish it will take a lot less time than if you left it in a mason jar. Freeze precipitate from naptha. Study some posts on this site for a good hour and I'm certain most of your questions will be answered There is almost zero color to the naptha. DMT is virtually insoluble in this aqueous phase, so it precipitates out of the naphtha solution via crystallization when kept Does this sound good then? put solvent in distilled water, shake, discard water You'd need to do a lot of extractions before you need to "wash" your naptha Reply reply UnorthodoxBuda • I know. Your naptha should be yellow and turn milky when disturbed. Robert DiGiovanni Robert DiGiovanni. I usually do 250g extractions but every time I look at the pulls in the dish before I put them in the freezer, the naphtha is yellow and when I take it out of the freezer the naphtha is still yellow (I have lots of crystals though) Does it make any difference? Pull the heptane up with a glass eyedropper, it should most likely get cloudy in the dropper, then put it into your collection jar/tray and freeze precip. Sometimes they will just be suspended in the naphtha, and will appear after you pour the naphtha Naphtha is not expected to undergo hydrolysis in the environment due to the lack of functional groups that hydrolyze under environmental conditions(3). Scraping is not an issue, because I recrystallize anyway. Welcome to the DMT-Nexus » WELCOME AREA (new members can post here) » FAQ - All your basic questions and answers » Why does the 24 hour naptha freeze help. how did they get there? why are those particles not precipitating during freezing?) comments sorted by Best Top New Controversial Q&A Add a Comment. Slowly pour off the naphtha without disturbing the crystals. A major source of naptha is crude oil, which is processed in refineries to break down the chains of hydrocarbons. A harm reduction focused subreddit for discussing the processes involved in the extraction of DMT along Naphtha is a concoction of hydrocarbons, some of which have quite high boiling points, making them harder to remove via evaporation alone. If its really saturated just put it in the freezer for a couple days. More posts you may like r/DMTlab. You should have evaped till it gets cloudy when you blow on it then freeze. part, where does the naptha go when you freeze it? and cant u just smoke the crystals straight out of the jar after theyve crystalized? Pull the heptane up with a glass eyedropper, it should most likely get cloudy in the dropper, then put it into your collection jar/tray and freeze precip. When naphtha is added, the DMT transfers into this nonpolar solution layer. I have a lot of naptha in a jar and have been trying to freeze precipitate the contents. So the DMT precipitates out of the naphtha solution as a solid crystal. A question I have is, if one were to use a cooler full of dry ice, would this work better? Someone I spoke with theorized that it Hier sollte eine Beschreibung angezeigt werden, diese Seite lässt dies jedoch nicht zu. And even when they don't leave any visual amounts of impurities i used 150g of MHRB in a solution of 150g lye and 3000ml water and 50 ml naptha for this pull (the bark was prepowdered) and im using normans tek i have just completed my first naptha pull (though it hasnt been frozen yet) I agitated 6 times allowing a 1-2 minutes for agitation, and then a full seperation afterwards. This will give you loads of very, very small pure white xtals. It's like how you can dissolve more sugar in hot water than you can cold. Pop the covered pyrex dish back into the freezer and leave alone overnight again. Naphtha freezes at -99°F (-72°C); however, a butane lighter won’t work when freezes because it won’t evaporate. 5% of the DMT has fallen out of solution) at this temperature? All the information available on the web does not seem very uniform. N,n-dmt is polymorphic. This saves naptha stinking out your freezer - granted you use extra naptha/or acetone but its a lot less Someone just attempted his first STB Tek and there are no crystals formed in his naptha after a night of freezing can anyone tell him what the problem is or what he can do www. ) One of the biggest downsides is the smell of naphtha . Coal tar also can be processed to yield this hydrocarbon, and it can be extracted from wood. So yea, nothing to worry about. ۩ Is the naptha cloudy in appearance when it has been in the freezer for some hours? If it is not cloudy then it is either very dilute or contains none or very little spice. Joined: 13-Apr Someone just attempted his first STB Tek and there are no crystals formed in his naptha after a night of freezing can anyone tell him what the problem is or what he can do The Chacruna Store Live plants. my naptha hasnt come out cloudy, does this You don't have to put it in the freezer. Grad_ster_ • I would advise against it but someone said use foil which I’d agree with cuz some of the Naptha might condensate on the lid and you wouldn’t want that as it’ll drip back down and it was Naptha on plastic so it could’ve picked some of it up Reply reply scoopskipotato11 • Naptha on foil is okay 326K subscribers in the DMT community. (1:5,,,1ml(or less) naphtha for every 5g mHRb) freezing produces cleaner product as well. If Deli-sliced meat and vacuum-sealed lunchmeat can last in the freezer up to one to two months, according to the U. New. It does not remove all impurities, heptane is still often better, but it can get rid of a good amount of them. Is it bad if I use my own fridge to freeze the naptha in the glass dish? So my fridge has 2 sides, one is a freezer and one is a fridge part. That was just from floaters. The fuel won’t be able to produce the necessary fuming cloud for ignition without evaporation. Controversial . FIRE -FIGHTING MEASURES Form: Liquid Flash point -typical: -21. Got slime instead of crystals after full 24hrs in freezer upvotes But this time around I used a little more naptha than usual & now my pint mason jars are like 3/4 of the way full. you can also reuse that naphtha, now that its not up in smoke. If warm naphtha can dissolve 2. [16] Naphthalene's chemical formula was determined by Michael Faraday in 1826. This is how Jet B is made. Collect in jar. Add a Comment. Boil large pot of water, and turn off and remove from heating surface. If you were to leave lighter fluid sitting on the charcoal without lighting it, then 100% of the fluid will have Well thats no emulsion you have there, it could be that the dark purplish tint of the mimosa migrated into the naptha tainting it. How long does it take for a solution of N,N-dimethyltryptamine & Naptha with 0ppm of impurity to freeze precipitate (until 99. E. SWIM is, however, unsure is his freezer is sufficiently cold to freeze precipitate and is worried about the smell permeating into the food. It would be a lot easier for me to leave it outside in the -10 to -25 degrees C weather than to clear shit out of my freezer. SWIM hasn't paid much attention to his temps but, he had one supplier that seemed excellent vs all others. But since I plan on using the same naphtha ad infinitum, I asked. . xSwishyy • Additional comment actions. You Yes sure it matters how saturated. tropane #1. Most technical grade solvents don't evaporate cleanly. Could swim make an aluminum foil pan sort of thing and pour the SWIM has been trying to freeze percip my naphtha for about 20 hours now, and while a few crystals did form, it was very very few. I am scared to filter through a coffee filter because I fear they will warm up and dissolve back into the naptha that will have soaked the paper and my dmt Step 4: Freeze Precipitation 3 5 7 10 Part 2: Methods of Purification 11 Section 1: Recrystallisation Section 2: Crystal Growing 11 14 Part 3: Salting 16 Section 1: Theory Section 2: Practical 16 17 Part 4: Making DMT Enhanced Leaf 21 Part 5: Methods of Ingestion 24 Suggestion 1: Smoking Enhanced Leaf Suggestion 2: Smoking Crystal Suggestion 3: Using Salts Suggestion 4: For example: Solubility: 10g of DMT/300mL Naphtha @ 25C 500mg of DMT/300mL Naphtha @ -10C (arbitrary value) When we freeze precipitate the DMT from the Naphtha, we would recover 9. Users browsing this Latex paints contain water, while oil paints contain an alkyd resin and a petroleum product, such as naphtha. Follow answered Oct 13, 2018 at 8:09. my naptha hasnt come out cloudy, does this Zote does not smell as nice as Fels-Naptha, but essential oils can be added, if you’d like. Du57mi73 wrote: I dont know what you mean by "as if i woulve vaporized the naptha in a more concentrated form first". I thought it was supposed to be yellowish Add lye, add mhrb, add naptha, separate, freeze. Expand user menu Open settings menu. On one hand, naphtha is relatively easy to find and easy to use. It has a 1:1 conversion-ratio. Your choice of materials really doesn´t matter. The naphtha can even clear quite a bit and loose a noticeable amount of the yellow discolouration. Top. Does VM&P Naphtha completely evaporate? If naphtha is used as a solvent, will it completely evaporate, or will it leave traces behind? It is pure naphtha, as indicated by the MSDS. 3. I'm sorry, what i mean is, do i have to Can’t pour off cold naptha after freeze precip because the dmt crystals are all loose from the glass. Joined: 13-Apr-2009. Log In / Sign Up; Advertise on Reddit; Shop Collectible Avatars; Get the Reddit app Scan this QR code solvent-refined heavy naphtha (petroleum) [3] 64742-48-9: 265-150-3: white spirit type 3: hydrotreated heavy naphtha (petroleum) [3] Physical properties. Posts: 65. Naphtha is a quite decent liquid insulator, with Thermal Conductivity rivaled only by Ethanol, Resin and liquefied gasses For the initial freeze precipitation, I always use a screw top jar, never a shallow dish. (It still has product in it. It was also kind of hard to tell though because of the frost on the glass. In fact it's way quicker to just evaporate it all . TheChacrunaStore. Does the freezer smell at all? Reply reply More replies More replies. If you just evaporate you'll have the spice plus the This question has been removed by our experts. So what's the point of something like noman's tek, which also uses lye and naptha, but a bunch of other stuff as well. Wait, why does everyone use Naptha when you can buy literal hexane on amazon? Extraction Question/Discussion Hexane is what makes up over half of naptha, and I've only read about how cleanly it evaporates. Naphtha does not contain chromophores that absorb at wavelengths >290 nm(3) and, therefore, is not expected to be susceptible to direct photolysis by sunlight(SRC). If it does give you the wisps when you blow on it and the freeze precip isn't working after 24 hours, you can evaporate some of the naptha, seal it back up and put it back in the freeze and try again. Last visit: 07-Jul-2024. They were of light color so not bits of bark. So assuming that those hydrocarbons were even present (Naphtha is a proprietary mixture), it wouldn't freeze as a Zote does not smell as nice as Fels-Naptha, but essential oils can be added, if you’d like. 3b) HARVEST Pour the naphtha but not the crystals out of the jar. The purer the product the less the "yield" is, whereas the impurer the product the more the "yield" seems. The How much naptha did you use per pull and how many pulls, and did you reduce (evap) your naptha after the pulls prior to freeze percip? Im just asking out of curiousty, and now to your question: From my knowledge i think cloudy solvent indicates that this solvent is saturated with DMT freebase and upon cooling, the solvent gets more and more cloudy because your I mean, it first uses lye, then naptha, then evaporates the naptha. Now put the lid back on your crystally mason jar and place it back into the freezer, upside down. Leave it in for 24 hours if you want- any longer you’re wasting your time. Before doing this in your garage, make sure there is no water in the mix, as frozen ice crystals will be present at much higher temperatures. my naptha hasnt come out cloudy, does this Welcome to the DMT-Nexus » THE DMT-NEXUS SITE » DMT Discussion » What do you recommend as the minimum naptha freeze-precip temp? What do you recommend as the minimum naptha freeze-precip temp? Options . I’ve done DMT extractions at least 15 times with MHRB. In some industries and regions, the name naphtha refers to crude oil or refined petroleum products such as kerosene or diesel fuel. Pour excess naptha out into a mason jar for future use. When put in the freezer even for 2-3 days the naptha just sits there and doesn't freeze evap or anything. Let the crystals and some rest naphtha dry by air (outside your room. What's the point of all that extra stuff, like a freezer, and amonia? Does lazyman's tek produce some different kind of dmt? Naphtha lighter fluid, commonly used in wick lighters and some starters, takes around 24 hours to evaporate, depending on the amount. Safety Data Sheet VM&P Naphtha Version 4. How long to freeze naphtha? #17213395 - 11/13/12 03:44 PM (11 years, 10 months ago) Edit : Reply : Quote : Quick Reply: I checked my jar this morning. swim wants to know because he just completed his first extraction and has the dmt saturated naphtha evaporating in drinking glasses but, the problem is he has no glass baking pans that he can use to make the process go faster. me STS is a community for people interested in growing, preserving and researching botanical species, particularly those with remarkable therapeutic and/or . Within 5 minutes the dmt will have crashed out of the naphtha. There is also some information suggesting that Fels Naptha can be used on your skin to treat Thinking of doing another extraction soon but to save space in my freezer I was thinking of putting all my pulls into one dish. if you store vodka in the freezer the water does not freeze and sink to the bottom. Let the rest of the naphtha fall down towards the lid. I have never seen or heard of this problem before, you could crank your freezer way way down like the other person said and leave it in there for a few days solid, but other then that my only other suggestion would be throw it out and start anew What do you recommend as the minimum naptha freeze-precip temp? Options . It can be yellow or white/clear, yet still be pure. Charcoal lighter fluid has another, slightly different chemical makeup. “Oil-based paint will freeze, but only in Good to hear all is going well Freeze time depends on how cold your freezer gets, if its super cold then it shouldnt need 3 days, but if you feel you have used slightly too much naphta, your solution wont be super saturated and the DMT will have a hard time crashing out. this warning needs to be propagated as even a badly secured jar-lid can lead to Naphtha does not freeze. This second freeze precip is re-x, or re-crystallisation. Hello Ive read so many places that naphtha turns into a milky white. e. With naphtha I would recommend you do a sodium carbonate wash and a plain water one before freeze precipitation. Please try exploring other questions in from our Ask and Answer section. In addition, do not forget the vagueness of the term "yield". 85°C (liquefaction point + 3 °C), Isoresin at 103 °C (liquefaction point + 3 °C. Is this going to affect the spice dropping out during a freeze precip because there is a lot of naptha this time around? Does it matter how saturated the naptha is? Will all of the spice still freeze precip properly & all fall out? First pull of clear naptha did not produce any, the 2nd pull with clear produced and everyone thereafter has so far. Posts: 169 . Is this going to affect the spice dropping out during a freeze precip because there is a lot of naptha this time around? Does it matter how saturated the naptha is? Will all of the spice still freeze precip properly & all fall out? But this time around I used a little more naptha than usual & now my pint mason jars are like 3/4 of the way full. The structure of two fused benzene rings was proposed by Emil Erlenmeyer in 1866, [17] and confirmed by SWIM is using a VM&P naptha based extract for MHRB. I ended up with 30mg of lovely looking (like that means anything!) very lightweight tiny crystals from a couple or 3 filters. Liquid - liquid extraction using Freeze precipitation does not generate smaller yields, this must be your friend's doing something wrong. After about Naphthalene is an organic compound with formula C. He saw white bumps about 3mm or so across in the bottom of the glass and took it out of the freezer and poured the naphtha out of the cup but the big white clumps sort of vanished. What he ends up doing is doing hot water baths and The freeze precipitation step calls for the DMT dissolved in naptha to be placed in a freezer to cause it to precipitate out. Sift out the broken glass, pour it all into some kind of tall glass jug (with all the water the PH will have gone down - less chance it will weaken the glass again) and let it separate It also wont freeze precipitate, and if you evaporate because of all the other stuff you pull together, it will probably be an oily result, not crystals. Can heptane be used in an A/B extraction as you would use naphtha? I. A little will stay trapped in the solvent. Place glass pie pan of Naptha over large pot of hot water. It is the simplest polycyclic aromatic hydrocarbon, and is a white crystalline solid with a characteristic odor that is detectable at Freeze precipitation Time: Sort answer: In most cases 12-24 hours is long enough. It has a thicker density than the Zippo lighters. Naptha will evaporate to desired amount within 15 to 30 minutes depending on how much excess Naptha you have. I thought The freeze precip was neccessary to force crystal growth. These two types of paint react very differently to cold weather. then I put it on its side with a fan pointed in the general direction for at least a few hours. I i used 150g of MHRB in a solution of 150g lye and 3000ml water and 50 ml naptha for this pull (the bark was prepowdered) and im using normans tek i have just completed my first naptha pull (though it hasnt been frozen yet) I agitated 6 times allowing a 1-2 minutes for agitation, and then a full i used 150g of MHRB in a solution of 150g lye and 3000ml water and 50 ml naptha for this pull (the bark was prepowdered) and im using normans tek i have just completed my first naptha pull (though it hasnt been frozen yet) I agitated 6 times allowing a 1-2 minutes for agitation, and then a full seperation afterwards. It depends on Naphtha (petroleum naphtha) is a generic term applied to refined, partly refined or unrefined crude oil products and liquid products of natural gas which distill below 240 °C (465 Aliphatic petroleum naphtha, Petroleum naphtha, Rubber solvent. The whole point is that naphtha should be as saturated as possible so that once the temperature goes down, naphtha will hold even less DMT so most will precipitate. Hier sollte eine Beschreibung angezeigt werden, diese Seite lässt dies jedoch nicht zu. How long does it take to evaporate the naphtha down to a reasonable level? And also would putting all my pulls into 1 dish cause more of a sticky/oily product as an end result? Hope to get some input from you guys I'm going to use KS vmp naphtha, and I am wondering how strong the fumes will Skip to main content. 5% of the DMT has fallen out of solution) at this temperature? i used 150g of MHRB in a solution of 150g lye and 3000ml water and 50 ml naptha for this pull (the bark was prepowdered) and im using normans tek i have just completed my first naptha pull (though it hasnt been frozen yet) I agitated 6 times allowing a 1-2 minutes for agitation, and then a full seperation afterwards. Valheim Genshin Impact Minecraft Pokimane Halo Infinite Call of Duty: Warzone Path of Exile Hollow Knight: Silksong Escape from Tarkov Watch Dogs: Legion. In the future, use less naphtha when you do your pulls. Pour it through a coffee filter and you're done. Try this for big xtals. Kerosene -type jet fuel (including Jet A and Jet A-1, JP-5, and JP-8) has a carbon number distribution between about 8 and 16 (carbon atoms per molecule); wide-cut or naphtha -type jet fuel oh man, that sucks I've had mason/bell jars do the same several times - highly basic solutions plus heat just destroys cheap glass. I was thinking a crock pot with a little bit of water set to low or medium might be ok, but im worried about heating it too much. Open menu Open navigation Go to Reddit Home. Posts: 169. I did a run and it turned out good but I tried to make a cart and wasted it all and kept some in the freezer and it turned out good. How can I go about evaporating maybe 100-150ml MATERIAL SAFETY DATA SHEET NAPHTHA Page 3 of 14 3 / 14 Notes to physician : Symptoms : Dizziness, Discomfort, Headache, Nausea, Kidney disorders, Liver disorders. burnt #4. endlessness, At what temp does naptha become polar, or more polar? I always used to use HOT naptha, but would always freeze precip after. What's the point of all that extra stuff, like a freezer, and amonia? Does lazyman's tek produce some different kind of dmt? By the way, if you do completely evaporate a batch of solvent, you should recrystallize the dmt afterwards in the normal freeze precipitation or with a slow evap to make sure that no naphtha is left in the product. Really oily, and it did not dry very well. Why does the 24 hour naptha freeze help: Options . Other say to just put the naphtha into a glass pyrex dish and let it evaporate. No recrystalizing. The SWIM follows Nomans Tek but after adding the Naptha and rolling the jar around repeatedly, the Naptha is clear. Q&A. Sort by: Best. Welcome to /r/DMT. NOTE: we need some new teks that fix a few common problems people are having The sludge I hear, can be fixed by adding the lye in slowly and making sure there is enough water The freeze precip problem can be fixed by not using so much naphtha during pulls Naphtha-type jet fuel: A fuel in the heavy naphtha boiling range having an average gravity of 52. You will be left with pure crystals in the bottom of your dish. 5-1. Any idea what cud be wrong? there's on a very thin layer (few mm) on the dish it's not like You aren’t evaporating the naphtha in the freezer- you are freeze precipitating the crystals out of it. Last I heard, he had decanted the naptha and was waiting for the remaining naptha to evaporate. (and remember DCM sinks and forms the bottom layer, it doesnt float like naphtha) Hexane and naphtha should be more or less similar The xtals you get from freeze pricipitating will all be very, very small. Posted : 8/7/2009 12:02:56 PM . You can evaporate the solvent down to half or a third before freezing though- that’s always helpful in getting the crystals to crash out of it You don't have to put it in the freezer. Some of the solvents in naphtha have melting point around -100C. The first 400g my Naptha was completely clear again There shouldn't be ANY frozen layer unless you pulled some of your water/lye layer over when you separated the Naptha. It's in the freezer right now so I'll see how it goes. But my question Skip to main content. 203 °C in the Spaced Out DLC), or Visco-Gel at 482. The naptha doesn't seem to be getting anything. Sustainable, ethically sourced, native American owned. [3] White spirit types 1–3 physical properties [1] Property T1: Low flash T2: Regular T3: I however experienced something new last time doing re-x. I don't have a very cold freezer but it will freeze preipitate spice from naptha. There was a At a certain point, the solvent would just freeze entirely. He proposed the name naphthaline, as it had been derived from a kind of naphtha (a broad term encompassing any volatile, flammable liquid hydrocarbon mixture, including coal tar). Posts: 3555. You didn't ruin it, just let it evap down almost all the way and then cover it with plastic wrap and leave it in the freezer for 12-24 hours. com ۩ #2. 2. But when naphtha is cold, very little DMT is able to stay dissolved. You could always try it out for yourself. You should start seeing something appear after an hour. “Clean the garden?” you might ask, scratching your head. (and remember DCM sinks and forms the bottom layer, it doesnt float like naphtha) Hexane and naphtha should be more or less similar A mixture of kerosene and naphtha will lower the freezing point. NFL 20 votes, 30 comments. Just wondering since naptha is so volatile that it stinks out peoples freezers, doesn’t some evaporate and condense on the plastic lid and possibly First time extracting - Im going to take my freezer naphtha dish out and drain the excess so I can start scraping that sweet spice from the bottom of the dish. no washing/cleaning steps to remove the remnants of the aqueous phase. Is this going to affect the spice dropping out during a freeze precip because there is a lot of naptha this time around? Does it matter how saturated the naptha is? Will all of the spice still freeze precip properly & all fall out? The naphtha freeze helps because there is a relationship between the temperature of the naphtha and how much DMT can dissolve in a given volume of naphtha. When I decide to get fresh naptha I evap all of my old stuff away and am able to collect a decent amount of product, though it's mixed with lots of plant fats and needs i used 150g of MHRB in a solution of 150g lye and 3000ml water and 50 ml naptha for this pull (the bark was prepowdered) and im using normans tek i have just completed my first naptha pull (though it hasnt been frozen yet) I agitated 6 times allowing a 1-2 minutes for agitation, and then a full seperation afterwards. swim knows the MHRB powder is good because he has done other extractions with it. I've found with a quick evap by fanning, it seems some naphtha can stay behind - like it is trapped between the tiny crystals that would form when you quickly evaporate Hi all! A friend has recently been in the middle of his first MHRB extraction and has officially put his naphtha in the freezer. You can also speed up crystallization if you put your naptha in i used 150g of MHRB in a solution of 150g lye and 3000ml water and 50 ml naptha for this pull (the bark was prepowdered) and im using normans tek i have just completed my first naptha pull (though it hasnt been frozen yet) I agitated 6 times allowing a 1-2 minutes for agitation, and then a full seperation afterwards. Also, it means the dmt is not very concentrated. Study some posts on this site for a good hour and I'm certain most of your questions will be answered sharetheseeds. Freeze precipitate means freezing the naphtha off so it “evaporates”, leaving only the DMT in The naphtha freeze helps because there is a relationship between the temperature of the naphtha and how much DMT can dissolve in a given volume of naphtha. What do? I’ve been using SVHT to process 500g of MHRB. Q&A [deleted] • Comment deleted by user. Naphtha is also Even if you are in a hurry to get your spice, you can always grab the crystals and either re-pull or just stick the naphtha right back in. Anyone know how much of a difference 5 degrees can Furthermore, the range of molecular mass between hydrocarbons (or different carbon numbers) is defined by the requirements for the product, such as the freezing point or smoke point. Posts: 6739. Posted : 4/26/2008 10:46:04 AM DMT-Nexus member. It is inflammable. I'd venture to say that the necessary defatting step was missed and It also wont freeze precipitate, and if you evaporate because of all the other stuff you pull together, it will probably be an oily result, not crystals. Swim even let the MHRB/Lye/Water solution sit for 3 hours before adding Naptha. The thing with that is he used a different freezer for freeze precipitation while using product from that vendor. Do you have a solution that's not crashing out? Blow some air on it. It's important to dry I'm not too good with freeze precips, & I think I know why - medium length story - anyroad up: I had some floaters, too, so I poured my naphtha through coffee filters & collected what got captured. He redissolved the goo in clean naptha and freeze precipitated it once again, with exceedingly good results compared to the prior turnout. Using a The naphtha can be saved and reused in future extractions. Again, this “recipe” doesn’t work well with HE washers , but Google can save you! If you do a search (using the term “homemade You used way too much naptha for the amount of mh you are using. Study some posts on this site for a good hour and I'm certain most of your questions will be answered codeofomerta, Read up on the subject matter. Crypto Evaporation removes solvent without affecting solute, so it increases the saturation of your solution. You will find clean white crystals forming on the glass If its not really saturatedevap it down and then put it in the freezer. Joined: 13-Mar-2008. the tryptamines are more soluble in naphtha at low temperatures, and as it contains high boiling/low melting hydrocarbons, so it's not suitable for temperatures as low as -78C. Get app Get the Reddit app Log In Log in to Reddit. does freeze precipitation work? Also, does heptane pull "jungle spice" alkaloids? I am going to be sharing this yield with a friend, and since will be his first time smoking DMT, I wanted to give him something more pure and traditional. 7% yields without a prevap, so I'm not Someone just attempted his first STB Tek and there are no crystals formed in his naptha after a night of freezing can anyone tell him what the problem is or what he can do sharetheseeds. Ive had success before using cys salt tek and gordo. IMO you've no In my experience, this naphtha has a yellow discoloration, probably from dissolved fats from the bark. It is used primarily for military turbojet and turboprop aircraft engines because it has a lower freeze point than other aviation Like other liquids, lighter fluid does freeze. me STS is a community for people interested in growing, preserving and researching botanical species, particularly those with remarkable therapeutic and/or psychoactive properties. Colorless liquid with a gasoline- or kerosene-like odor. Plus you will get all the dmt out of the solvent this way. Not to mention DCM seems to be carcinogenic, be careful. ygohd yikwnm eewzq dcfq wmkt rowrr adnz hrboal ymxiz gjsamar